New horizon in mechanochemistry—high-temperature,high-pressure mechanical synthesis in a planetary ball mill—with magnesium hydride synthesis as an example

A new route of materials synthesis, namely, high-temperature, high-pressure reactive planetary ball milling (HTPRM), is presented. HTPRM allows for the mechanosynthesis of materials at fully controlled temperatures of up to 450 °C and pressures of up to 100 bar of hydrogen. As an example of this application, a successful synthesis of magnesium hydride is presented. The synthesis was performed at controlled temperatures (room temperature (RT), 100, 150, 200, 250, 300, and 325 °C) while milling in a planetary ball mill under hydrogen pressure ($>$50 bar). Very mild milling conditions (250 rpm) were applied for a total milling time of 2 h, and a milling vial with a relatively small diameter (φ = 53 mm, V = ～0.06 dm³) was used. The effect of different temperatures on the synthesis kinetics and outcome were examined. The particle morphology, phase composition, reaction yield, and particle size were measured and analysed by scanning electron microscopy, X-ray diffraction, differential scanning calorimetry (DSC) techniques. The obtained results showed that increasing the temperature of the process significantly improved the reaction rate, which suggested the great potential of this technique for the mechanochemical synthesis of materials.     

Magnetic Properties of Fe-Doped Rutile

Ball-milling method was applied to dissolve Fe into titanium dioxide (TiO₂). X-ray diffraction indicated the starting anatase changed to a rutile-type structure with oxygen deficiency after ball milling. Transmission electron microscopy and X-ray absorption experiments were conducted to examine the possible existence of magnetic impurities in the ball-milled powders after they were leached in HCl solutions. Temperature dependence of the resistivity shows semiconducting behavior and the magnetic hysteresis loops at 5 and 300 K exhibit ferromagnetic characteristics. Fe-doped TiO₂ films were also prepared by pulsed laser deposition. The magnetic properties of the films are discussed.     

Precision equipment for symmetrical bending— Part 1. The loading system

The design and performance of precision bending equipment for testing straight beams with constant rectangular section under a pure bending moment is described. Part 1 deals with the loading arrangements and Part 2 with the rig for measuring beam deflection. The methods for recording deflection of strain gauges applied on the beam have been described elsewhere.^1–4
The reactions to the deadweight gravity loads are taken via ball bearings. The total bending moment inaccuracy, i.e. the sum of estimated systematic errors and random errors, the latter expressed as the 2Ga confidence interval about the mean (2G_cim), is about ± 25 x. 10^-4%, for 23 tests with a steel beam with 15 mm × 75 mm cross sectional dimensions, loaded to 1-1.5 mm/m strain.
The measuring rig stands on the beam via hardened and polished spherical segment feet and uses a capacitive transducer system with less than 5nm resolution. Various application tasks are described. The total inaccuracy of the measured deflection, i.e. apart from bending moment inaccuracy, is about ± 35 times 10^4% for about 10 reproduced, not repeated, tests with the same steel beam. The deflection for such a beam is of the order of 2 to 4 mm.     

挡渣球和挡渣塞技术在转炉炼钢的应用

介绍了档渣球和挡渣塞技术在转炉炼钢的实际应用，有利于降低原材料消耗、增加企业效益。     

东方N-18250-2型凝汽器胶球清洗系统改造

对湘潭电厂存在已久的胶球清洗装置收球率低的问题进行了深入探讨，结合电厂对胶球清洗系统的改造、试验过程，分析并提出了影响胶球清洗装置清洗效果及收球率的诸多原因及其解决方法。     

机械合金化的原理及在磁性材料研究中的应用

介绍了机械合金化的原理和描述机械合金化过程的理论模型。综述了机械合金化在磁性材料研究中的应用，并对目前研究中的存在的问题及发展前景进行了分析。     

基于OpenGL五轴联动数控仿真系统碰撞干涉检验实时仿真技术及算法研究

介绍了Com-5NCSS五轴联动数控仿真系统运用的“实时仿真”技术，在此基础上提出基于规则实体表面网格化遍历的八叉树单球组合模型，该模型应用于Com-5NCSS仿真系统中，实现了碰撞干涉的快速检测，满足了数控仿真系统的“实时性”要求。     

轴向进给比对薄壁管滚珠旋压影响的有限元分析

通过有限元数值模拟方法得出滚珠旋压中薄壁管在不同凹模旋转速度条件下轴向进给比的变化规律及工件的成形规律,并对模拟结果的等效应变分布做了分析,并与实验结果进行比较,给出薄壁管滚珠旋压时进给比的选取范围.结果表明,进给比对滚珠旋压中薄壁管直径的胀缩和工件的质量有着显著的影响.另外,从计算的模具所受的三向载荷变化情况分析了模具的使用寿命.     

关于粉体成球机盘体几何形状的研究

通过对粉体小球在粉体成球机盘底上运动轨线的研究,利用Euler定理,结合其参数特点,得到了不同几何形状的盘底在成球过程中对粉体小球运动的影响,球面盘底较平面盘底更有利于成球的结论。     

磨机大齿轮对缝处产生张口的初探

针对大中型磨机大齿轮对缝处在使用中会产生张口现象而降低其使用寿命的问题,从分析产生张口的原因入手,通过理论计算,提出设计的配合间隙,并指出在安装与使用中应注意的问题.